Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass

Shivanand Yallappa Adaganti; Basavaraj Mahipat Kulkarni; Gururaj Pandurang Desai; Shivappa Shanmukhappa

doi:doi:10.11648/j.ijrse.20140301.11

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Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass

Shivanand Yallappa Adaganti, Basavaraj Mahipat Kulkarni, Gururaj Pandurang Desai, Shivappa Shanmukhappa

Published in International Journal of Renewable and Sustainable Energy (Volume 3, Issue 1)

Received: 23 October 2013 Published: 20 December 2013

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Abstract

Biomass has been pretreated by hydrothermal explosion using different experimental conditions of temperature between 135 and 173°C and operating time of 45 minutes. The effects of hydrothermal explosion conditions have been investigated by measuring chemical compositions (cellulose, hemicelluloses and lignin) in Calliandra calothyrsus. Hydrothermal explosion pretreatment removes the major part of the hemicelluloses, and makes the high cellulose in the solid material for further enzyme hydrolysis. At severity factor of (log Ro) 3.82 (173oC, 7.5 bar, 45 min), the biomass fibers contained the significant lowest hemicelluloses and the highest of celluloses at 4.82 % DW and 58.26 % DW, respectively. Since Calliandra calothyrsus has higher lignin content, lignin structure might be resisting hemicelluloses degradation by hydrothermal explosion pretreatment. Therefore, hydrothermal explosion of lignocellulosic materials to remove hemicelluloses might significantly enhance the efficiency of cellulose hydrolysis.

Published in	International Journal of Renewable and Sustainable Energy (Volume 3, Issue 1)
DOI	10.11648/j.ijrse.20140301.11
Page(s)	1-5
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2013. Published by Science Publishing Group

Keywords

Calliandra Calothyrsus, Hydrothermal Explosion, Chemical Compositions

References

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[7]	Heitz M., Capek-Ménard E., Koeberle P., Cagné J., Chornet E., Fractionation of Populus tremuloides at the pilot plant scale: optimization of steam pretreatment conditions using the Stake II technology, Bioresource Technology, 1991, 35, 23 - 32.
[8]	TAPPI Standard, T 204 cm-07, Solvent extractives of wood and pulp, 1998 TAPPI Standard T 222 om-06, Acid insoluble lignin in wood and pulp, 2011 TAPPI Standard T 257 cm-02, Sampling and preparing wood for analysis, 2002
[9]	Goering H. K., and Van Soest P.J., Forage Fiber Analysis (Apparatus, Reagents, Prosedures and some Applications),United States Department of Agriculture (USDA) 1970, Agricultural Handbook No. 379: 20
[10]	Ballesteros I.,Oliva J.M., Negro M.J., Manzanares P., and Ballesteros M., Enzymatic hydrolysis of steam exploded herbaceous agricultural waste (Brassica carinata) at different particles sizes, Process Biochem. 2002, 38(2), 187-192
[11]	Sun X.F., Xu F., Sun R.C., Fowler P., and Baird M.S., Characteristics of degraded cellulose obtained from steam-exploded wheat straw, Carbohyd. Res. 2005, 340(1), 97-106.
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[13]	Jonoobi M., Harun J., Shakeri A., Misra M., and Oksman K., Chemical composition,crystallinity and thermal degradatuion of bleached and unbleached kenaf bast (Hibiscus cannabinus) pulp and nanofibers, Bioresources,2009,4(2),626-639

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Shivanand Yallappa Adaganti, Basavaraj Mahipat Kulkarni, Gururaj Pandurang Desai, Shivappa Shanmukhappa. (2013). Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass. International Journal of Sustainable and Green Energy, 3(1), 1-5. https://doi.org/10.11648/j.ijrse.20140301.11

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ACS Style

Shivanand Yallappa Adaganti; Basavaraj Mahipat Kulkarni; Gururaj Pandurang Desai; Shivappa Shanmukhappa. Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass. Int. J. Sustain. Green Energy 2013, 3(1), 1-5. doi: 10.11648/j.ijrse.20140301.11

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Shivanand Yallappa Adaganti, Basavaraj Mahipat Kulkarni, Gururaj Pandurang Desai, Shivappa Shanmukhappa. Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass. Int J Sustain Green Energy. 2013;3(1):1-5. doi: 10.11648/j.ijrse.20140301.11

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@article{10.11648/j.ijrse.20140301.11,
  author = {Shivanand Yallappa Adaganti and Basavaraj Mahipat Kulkarni and Gururaj Pandurang Desai and Shivappa Shanmukhappa},
  title = {Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass},
  journal = {International Journal of Sustainable and Green Energy},
  volume = {3},
  number = {1},
  pages = {1-5},
  doi = {10.11648/j.ijrse.20140301.11},
  url = {https://doi.org/10.11648/j.ijrse.20140301.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijrse.20140301.11},
  abstract = {Biomass has been pretreated by hydrothermal explosion using different experimental conditions of temperature between 135 and 173°C and operating time of 45 minutes. The effects of hydrothermal explosion conditions have been investigated by measuring chemical compositions (cellulose, hemicelluloses and lignin) in Calliandra calothyrsus. Hydrothermal explosion pretreatment removes the major part of the hemicelluloses, and makes the high cellulose in the solid material for further enzyme hydrolysis. At severity factor of (log Ro) 3.82 (173oC, 7.5 bar, 45 min), the biomass fibers contained the significant lowest hemicelluloses and the highest of celluloses at 4.82 % DW and 58.26 % DW, respectively. Since Calliandra calothyrsus has higher lignin content, lignin structure might be resisting hemicelluloses degradation by hydrothermal explosion pretreatment. Therefore, hydrothermal explosion of lignocellulosic materials to remove hemicelluloses might significantly enhance the efficiency of cellulose hydrolysis.},
 year = {2013}
}

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TY  - JOUR
T1  - Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass
AU  - Shivanand Yallappa Adaganti
AU  - Basavaraj Mahipat Kulkarni
AU  - Gururaj Pandurang Desai
AU  - Shivappa Shanmukhappa
Y1  - 2013/12/20
PY  - 2013
N1  - https://doi.org/10.11648/j.ijrse.20140301.11
DO  - 10.11648/j.ijrse.20140301.11
T2  - International Journal of Sustainable and Green Energy
JF  - International Journal of Sustainable and Green Energy
JO  - International Journal of Sustainable and Green Energy
SP  - 1
EP  - 5
PB  - Science Publishing Group
SN  - 2575-1549
UR  - https://doi.org/10.11648/j.ijrse.20140301.11
AB  - Biomass has been pretreated by hydrothermal explosion using different experimental conditions of temperature between 135 and 173°C and operating time of 45 minutes. The effects of hydrothermal explosion conditions have been investigated by measuring chemical compositions (cellulose, hemicelluloses and lignin) in Calliandra calothyrsus. Hydrothermal explosion pretreatment removes the major part of the hemicelluloses, and makes the high cellulose in the solid material for further enzyme hydrolysis. At severity factor of (log Ro) 3.82 (173oC, 7.5 bar, 45 min), the biomass fibers contained the significant lowest hemicelluloses and the highest of celluloses at 4.82 % DW and 58.26 % DW, respectively. Since Calliandra calothyrsus has higher lignin content, lignin structure might be resisting hemicelluloses degradation by hydrothermal explosion pretreatment. Therefore, hydrothermal explosion of lignocellulosic materials to remove hemicelluloses might significantly enhance the efficiency of cellulose hydrolysis.
VL  - 3
IS  - 1
ER  -

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Author Information

Shivanand Yallappa Adaganti

Chemical Engineering Department, SDM College of Engineering and Technology, Dharwad, Karnataka, India
Basavaraj Mahipat Kulkarni

Chemical Engineering Department, Bapuji Institute of Engineering and Technology, Davangere, Karnataka, India
Gururaj Pandurang Desai

Chemical Engineering Department, Bapuji Institute of Engineering and Technology, Davangere, Karnataka, India
Shivappa Shanmukhappa

Chemical Engineering Department, Bapuji Institute of Engineering and Technology, Davangere, Karnataka, India

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APA Style

Shivanand Yallappa Adaganti, Basavaraj Mahipat Kulkarni, Gururaj Pandurang Desai, Shivappa Shanmukhappa. (2013). Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass. International Journal of Sustainable and Green Energy, 3(1), 1-5. https://doi.org/10.11648/j.ijrse.20140301.11

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ACS Style

Shivanand Yallappa Adaganti; Basavaraj Mahipat Kulkarni; Gururaj Pandurang Desai; Shivappa Shanmukhappa. Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass. Int. J. Sustain. Green Energy 2013, 3(1), 1-5. doi: 10.11648/j.ijrse.20140301.11

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AMA Style

Shivanand Yallappa Adaganti, Basavaraj Mahipat Kulkarni, Gururaj Pandurang Desai, Shivappa Shanmukhappa. Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass. Int J Sustain Green Energy. 2013;3(1):1-5. doi: 10.11648/j.ijrse.20140301.11

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@article{10.11648/j.ijrse.20140301.11,
  author = {Shivanand Yallappa Adaganti and Basavaraj Mahipat Kulkarni and Gururaj Pandurang Desai and Shivappa Shanmukhappa},
  title = {Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass},
  journal = {International Journal of Sustainable and Green Energy},
  volume = {3},
  number = {1},
  pages = {1-5},
  doi = {10.11648/j.ijrse.20140301.11},
  url = {https://doi.org/10.11648/j.ijrse.20140301.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijrse.20140301.11},
  abstract = {Biomass has been pretreated by hydrothermal explosion using different experimental conditions of temperature between 135 and 173°C and operating time of 45 minutes. The effects of hydrothermal explosion conditions have been investigated by measuring chemical compositions (cellulose, hemicelluloses and lignin) in Calliandra calothyrsus. Hydrothermal explosion pretreatment removes the major part of the hemicelluloses, and makes the high cellulose in the solid material for further enzyme hydrolysis. At severity factor of (log Ro) 3.82 (173oC, 7.5 bar, 45 min), the biomass fibers contained the significant lowest hemicelluloses and the highest of celluloses at 4.82 % DW and 58.26 % DW, respectively. Since Calliandra calothyrsus has higher lignin content, lignin structure might be resisting hemicelluloses degradation by hydrothermal explosion pretreatment. Therefore, hydrothermal explosion of lignocellulosic materials to remove hemicelluloses might significantly enhance the efficiency of cellulose hydrolysis.},
 year = {2013}
}

Copy | Download

TY  - JOUR
T1  - Effect of Hydrothermal Explosion Pretreatment on the Composition and Structure of Calliandra Calothyrsus Shrub – a Lignocellulosic Biomass
AU  - Shivanand Yallappa Adaganti
AU  - Basavaraj Mahipat Kulkarni
AU  - Gururaj Pandurang Desai
AU  - Shivappa Shanmukhappa
Y1  - 2013/12/20
PY  - 2013
N1  - https://doi.org/10.11648/j.ijrse.20140301.11
DO  - 10.11648/j.ijrse.20140301.11
T2  - International Journal of Sustainable and Green Energy
JF  - International Journal of Sustainable and Green Energy
JO  - International Journal of Sustainable and Green Energy
SP  - 1
EP  - 5
PB  - Science Publishing Group
SN  - 2575-1549
UR  - https://doi.org/10.11648/j.ijrse.20140301.11
AB  - Biomass has been pretreated by hydrothermal explosion using different experimental conditions of temperature between 135 and 173°C and operating time of 45 minutes. The effects of hydrothermal explosion conditions have been investigated by measuring chemical compositions (cellulose, hemicelluloses and lignin) in Calliandra calothyrsus. Hydrothermal explosion pretreatment removes the major part of the hemicelluloses, and makes the high cellulose in the solid material for further enzyme hydrolysis. At severity factor of (log Ro) 3.82 (173oC, 7.5 bar, 45 min), the biomass fibers contained the significant lowest hemicelluloses and the highest of celluloses at 4.82 % DW and 58.26 % DW, respectively. Since Calliandra calothyrsus has higher lignin content, lignin structure might be resisting hemicelluloses degradation by hydrothermal explosion pretreatment. Therefore, hydrothermal explosion of lignocellulosic materials to remove hemicelluloses might significantly enhance the efficiency of cellulose hydrolysis.
VL  - 3
IS  - 1
ER  -

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